HPTLC ATLAS

 

Botanical Information Angelica acutiloba (Siebold & Zucc.) Kitag.

Synonyms Angelica acutiloba var. sugiyamae Hikino
Angelica acutiloba var. tsukubana Hikino
Apium ternatum Siebold Verh. Batav. .
Ligusticum acutilobum Siebold & Zucc.
Sium triternatum Miq.
Common name (ja) トウキ
Common name (ko) 일당귀
Common name (vi) Đương quy Nhật Bản
Common name (zh) 东当归

Sample preparation Mix 1.0 g of powdered sample with 5.0 mL of methanol and shake for 10 min, then centrifuge the solution and use the supernatant as test solution
Mobile phase Toluene, ethyl acetate, acetic acid 90:10: 1 (v/v/v)
Derivatization Spray with 10% sulfuric acid in methanol, then heat the plate at 100°C for 3 min
System Suitability Test (SST) Under UV 366 nm prior to derivatization
  • Imperatorin: green fluorescent zone RF ~ 0.33
  • Osthole: blue fluorescent zone RF ~ 0.38
  • Isoimperatorin: green fluorescent zone RF ~ 0.44
HPTLC Chromatograms (different origin(s))
HPTLC Chromatograms (related drug(s))
ATLAS documents ATLAS Method document
Image comparison of Angelica acutiloba
Image comparison of Angelica acutiloba and different varieties
Image comparison of Angelica acutiloba and related herbal drugs
visionCATS data (CAMAG software)

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