Botanical Information Angelica dahurica (Hoffm.) Benth. & Hook.f. ex Franch. & Sav.
Synonyms | Angelica dahurica var. pai-chi Kimura |
Angelica glabra (Y.Yabe) Makino | |
Angelica macrocarpa H.Wolff Repert. | |
Angelica porphyrocaulis Nakai & Kitag. | |
Angelica porphyrocaulis f. latisecta Kitag. | |
Angelica pubescens var. glabra Y.Yabe | |
Angelica tschiliensis H.Wolff | |
Callisace dahurica Hoffm. | |
Thysselinum davuricum (Hoffm.) Spreng. | |
Common name (en) | Dahurian angelica |
Common name (de) | Sibirische Engelwurz |
Common name (fr) | Angélique dahurica |
Common name (ko) | 백지 |
Common name (th) | แปะจี้ |
Common name (vi) | Bạch chỉ |
Common name (zh) | 白芷 |
Sample preparation | Mix 1.0 g of powdered sample with 5.0 mL of methanol and shake for 10 min, then centrifuge the solution and use the supernatant as test solution |
Mobile phase | Toluene, ethyl acetate, acetic acid 90:10: 1 (v/v/v) |
Derivatization | Spray with 10% sulfuric acid in methanol, then heat the plate at 100°C for 3 min |
System Suitability Test (SST) | Under UV 366 nm prior to derivatization
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HPTLC Chromatograms |
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HPTLC Chromatograms |
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ATLAS documents |
ATLAS Method document Image comparison of Angelica dahurica Image comparison of Angelica dahutrica and related herbal drugs visionCATS data (CAMAG software) |
Sample preparation | To 1 g of the freshly powdered herbal drug add 4 mL of heptane, close and sonicate for 5 min. Centrifuge the mixture and use the supernatant |
Mobile phase | Acetic acid, ethyl acetate, toluene 1:10:90(v/v/v) |
Derivatization | No derivatization |
Sample preparation | To 0.5 g of the powder add 10 mL of ether, soak for 1 hour and shake frequently, filter, evaporate the filtrate to dryness, dissolve the residue in 1 mL of ethyl acetate as test solution |
Mobile phase | Petroleum ether (30-60°C), ether 3:2 (v/v) |
Derivatization | No derivatization |
Sample preparation | Add 2.0 g of powdered sample to 10 mL of methanol, ultrasonicate for 30 min, filter and use the filtrate |
Mobile phase | Petroleum ether (30-60°C), ether 3:2 (v/v) |
Derivatization | No derivatization |
Sample preparation | Reflux 1 g of the powdered sample with 10 mL of dichloromethane for 30 minutes and filtering. Evaporate the filtrate to dryness. Dissolve the residue in 1 mL of toluene |
Mobile phase | Toluene, ethyl acetate, acetic acid 75:25:5 (v/v/v) |
Derivatization | Spray with a 5% (w/v) solution of potassium hydroxyde |
Sample preparation | 5 g coarsely ground drug are soxhlet-extracted with 50 mL n-hexane for one hour. The extract is evaporated to dryness and redissolved in 2.5 mL ethanol and filtered |
Mobile phase | Toluene, ethyl acetate, acetic acid 90:10:1 (v/v/v) |
Derivatization | Spray with anisaldehyde reagent, and heat the plate at 100°C for 5-10 min |